Mô tả

Introduction:

Gas Absorption is one of the very first Mass Transfer Unit Operations studied in early process engineering. It is very important in several Separation Processes, as it is used extensively in the Chemical industry.

Understanding the concept behind Gas-Gas and Gas-Liquid mass transfer interaction will allow you to understand and model Absorbers, Strippers, Scrubbers, Washers, Bubblers, etc...

We will cover:

  • REVIEW: Of Mass Transfer Basics required

  • GAS-LIQUID interaction in the molecular level, the two-film theory

  • ABSORPTION Theory

  • Application of Absorption in the Industry

  • Counter-current & Co-current Operation

  • Several equipment to carry Gas-Liquid Operations

  • Bubble, Spray, Packed and Tray Column equipments

  • Solvent Selection

  • Design & Operation of Packed Towers

  • Pressure drop due to packings

  • Design & Operation of Tray Columns

  • Single Component Absorption

  • Single Component Stripping/Desorption

  • Diluted and Concentrated Absorption

  • Basics: Multicomponent Absorption

  • Software Simulation for Absorption/Stripping Operations (ASPEN PLUS/HYSYS)

Solved-Problem Approach:

All theory is backed with exercises, solved problems, and proposed problems for homework/individual study.

At the end of the course:

You will be able to understand mass transfer mechanism and processes behind Absorption and Stripping. You will be able to continue with a Distillation Theory and more Mass Transfer Unit Operation Course and/or Separation Processes Course.

About your instructor:

I majored in Chemical Engineering with a minor in Industrial Engineering back in 2012.

I worked as a Process Design/Operation Engineer in INEOS Koln, mostly on the petrochemical area relating to naphtha treating. There I designed and modeled several processes relating separation of isopentane/pentane mixtures, catalytic reactors and separation processes such as distillation columns, flash separation devices and transportation of tank-trucks of product.

Bạn sẽ học được gì

Understand the principle behind gas Absorption and Stripping

Design & Operate Packed Towers

Design & Operate Tray Columns

Calculate the required values for a given Separation Process using Absorption/Stripping

Solve analytically via Kremser Brown Souders Equation

Understand the concept of "operation line" and "equilibrium line"

Calculate the total required stages via Graphical Method

Learn about Absorption Column Equipment (Trays, Packings, Column Internals)

Calculate & Understand the minimum L/G ratio

The HETP method for Packings

The MTU, Method of Transfer Units for Packed Towers

Model Co-Current and Counter-Current Operations

Solve relevant problems involving Gas Absorption and Stripping

Yêu cầu

  • Mass Transfer Basics
  • Transport Phenomena (Recommended)
  • Thermodynamics
  • Mass and Energy Balances
  • Physical Chemistry

Nội dung khoá học

8 sections

Introduction

5 lectures
Welcome to the Course!
05:41
Introduction
05:16
Requirements
04:49
Recommended Public
03:49
Reference Material
02:45

Mass Transfer Review

34 lectures
Section 2 - Introduction
02:26
2.1 Equilibrium
00:29
What is Equilibrium?
03:36
Vapor Pressure
04:55
Partial Pressure
02:38
Raoult’s Law
05:17
Gas Solubility in Liquids - Overview
05:25
Gas Solubility Analysis
02:49
Henry’s Law
06:48
2.2 Diffusion & Convection
00:45
What is Flux?
09:05
What is Ja? Diffusion Flux
02:42
What is Diffusion?
06:48
Fick's Law
04:56
Engineering Applications for Diffusion
03:21
Case A - Equimolar Counter-Difussion (EMD)
06:45
Exercise#01 - EMD
14:04
Case B - Unimolecular Diffusion (UMD)
16:27
Exercise#02 - UMD
06:31
Convection
04:38
2.3 Interphase Mass Transfer
01:12
Equilibrium Distribution Curve
06:08
Film Concept
05:05
Two-Film Theory
06:08
Two-Film Theory and Equilibrium Solubility Curve
08:53
Analysis of Mass Transfer Process using Two-Film Theory
05:46
Film MT Coefficients
07:50
Local MTC: kx, ky
03:27
Mass Transfer Coefficients & Correlations
03:31
Overall Mass Transfer Coefficients
06:29
Local vs. Overall (MTC)
03:23
Mass Transfer Resistance
02:35
Analysis of Gas Solubility
04:44
Section 2 - Closure
00:56

Gas Absorption

26 lectures
Introduction to Gas Absorption
01:13
What is Absorption?
08:32
Nomenclature in Absorption
02:58
Gas Absorption Examples
09:25
Physical vs. Chemical Absorption
02:34
Scope of the Course
03:53
Desorption & Stripping
03:08
Stripping Examples
03:38
Case Study - Amine Gas Treating AKA Sweetening Sour Gas
09:20
Equipment & Operation (Absorption and Stripping)
04:10
Type of Equipment - Dispersion of Gas-Liquid and Liquid-Gas
04:12
Spray Column
02:36
Bubble Column
02:00
Packed Column Intro
01:32
Tray Column Intro
01:25
Design Steps
06:27
Solvent Selection
01:40
Solvent Selection - Gas Solubility
02:28
Solvent Selection - Volatility
00:58
Solvent Selection - Corrosiveness
00:45
Solvent Selection - Cost
01:09
Solvent Selection - Viscosity
01:19
Solvent Selection - Safety
01:00
Types of Operations
01:39
Single vs. Multiple Stages
08:28
Gas Absorption Closure
00:46

Tray Column - Absorbers

70 lectures
Section 4 - Introduction
04:22
4.1 Introduction to Tray Columns
00:58
Introduction to Tray Columns
04:18
4.2 Equipment used in Tray Columns
01:22
Sieve Trays
04:08
Valve Trays
03:57
Bubble Cap Trays
03:39
Tray Considerations
00:27
Trays - Spacing
02:28
Trays - Sizing
01:12
Trays - Layouts
04:48
Trays - Materials
02:50
Trays - Manways
01:30
Trays - Operations
01:37
Tray - Pressure Drop
01:27
Trays - Costs
01:07
Tray - Maintenance
00:53
Trays - Summary
01:04
All other Pieces
00:27
Bubbling Area
01:43
Contact Area
01:24
Weir
02:34
Downcomer
03:54
4.3 Design & Model
00:23
Counter-current Operation
05:47
Counter-current Operation for Dilute Systems
05:47
Operation Line
04:40
Exercise#03 - Operation Line
05:54
Equilibrium Line
04:09
Plotting both Lines
06:11
Min. Solvent Flow Rate
12:23
Exercise#04 - Min. Liquid Flow Rate
05:51
Exercise#05: Analytical Lmin
13:33
Other Cases
01:22
Co-Current Operation
01:53
Counter-Current Gas Stripping
01:39
4.4 Number of Equilibrium Stages
01:18
Nomenclature used in Gas Absorption
06:30
Graphical Method - McCabe Thiele
05:33
Exercise#06 - Graphical Method
13:48
The Dilute Absorption Factor "A"
01:25
Analytical Method - Kremser Equation
03:16
Exercise#07 - Kremser Equation
04:46
Exercise#08: Kremser vs. Graphical
03:58
Dynamic Simulation - Absorption Column
07:26
Dynamic Simulation - Stripping Column
04:09
Exercise#09 - Absorption (mass fraction)
09:56
Stage Efficiency
05:44
Murphree's Efficiency
03:30
Examples of real industrial process stage efficiencies
01:44
Exercise#10: Stage & Murphree Efficiencies
02:53
Exercise#11: Gas Absorber & Murphree Efficiencies
11:50
Column Operation
02:51
Column Operation - Normal
02:04
Column Operation - Flooding
03:41
Column Operation - Priming
02:26
Column Operation - Coning
01:43
Column Operation - Weeping
01:47
Column Operation - Dumping
03:37
Column Operation - Summary
03:34
Tray Diameter Introduction
06:14
Tray Spacing
02:25
Exercise#12: Diameter of a Tray Column
13:58
Pressure Drop in Trays
03:49
Hd, Dry Liquid sieve loss - Pressure Drop in trays
03:07
Hl, (equivalent h eight of clear liquid holdup)
03:39
Hd, Surface Tension Pressure loss
01:17
Exercise#13: Pressure Drop in a Tray Columns
11:25
Summary of Exercises 11, 12 and 13
04:42
Section 3 - Closure
00:46

Packed Column - Absorbers

48 lectures
Introduction to Packed Columns
02:06
5.1 Intro to Packed Towers
01:51
Approach to Design
02:29
5.2 Equipment in Packed Columns
00:20
Packed Columns vs. Tray Columns
05:03
Introduction to Packings
04:05
Packing Material
02:26
Random Packing
01:28
Stacked Packing
01:39
Structural Packing
00:58
Other Column Internals
01:51
Liquid distributor
02:13
Liquid/Vapour Re-Distributor
01:07
Vapour Distributor
01:12
Demister / Mist Eliminator
01:45
Vortex breaker
00:48
Packing Supports
01:23
Retaining devices (Hold-down Plate & Bed limiter )
01:07
Column Structure - Top
01:23
Column Structure - Middle
01:44
Column Structure - Bottom
10:33
5.3 Design & Model
02:32
Introduction to Column Diameters & Pressure Drop
03:51
Analysis of Drop in Pressure in Packed Towers
07:53
Flow Parameter vs. Pressure Drop Parameters - Graph
04:08
Flow Parameter vs. Pressure Drop Parameter - Equation
01:36
Flooding Pressure Drop Correlation
01:49
Method 1: Fractional Approach to Flooding Gas Velocity (Absorber Diameter)
04:35
Method 2: Maximum Pressure Drop Approach (Absorber Diameter)
07:35
Exercise#14 - Drop in Pressure due to Packings
12:55
Exercise#15: Pressure drop in a Packed Column
06:58
Exercise#16: Pressure Drop in an Ethanol Absorber (50mm Hiflow Metallic Rings)
11:48
HETP (Height Equivalent to a Theoretical Plate)
10:14
Exercise#17 - HETP
02:03
Exercise#18 - HETP
04:39
Method of Transfer Units
04:34
Number of Transfer Units (NTU)
01:25
Height of Transfer Unit (HTU)
02:11
Overall vs. Local Mass Transfer coefficients in MTU
03:00
Gas Phase - Method of Transfer Units MTU
04:22
Liquid Phase - Method of Transfer Units MTU
02:13
Exercise#19 - Mass Transfer Units Method in a Packed Columns
06:14
Steps - Method of Transfer Units MTU
02:31
HETP vs MTU
03:48
Exercise#20: Mass Transfer Units Design
06:45
Exercise#21 Packed Column Height increase due to increase in purity
04:40
Exercise#22 Packing Height: Acetone-Air-Water
06:14
Section 5 - Closure
02:32

Advanced Systems

11 lectures
Introduction to Section 6
02:39
Non-diluted Cases in Tray Columns
07:46
Exercise#23 Concentrated Tray Column Absorber
11:04
Packed Columns in Non-diluted Cases
01:35
Exercise#24 Concentrated Case - Packed Column
11:20
6.2 Multicomponenet Absorption
05:20
Methodology for Multicomponent Absorption
06:16
Case Study - Multicomponent Absorption
15:22
Sum-Rates (SR) Method for Absorption and Stripping
09:38
6.3 Reactive Absorption
04:06
Section 6 - Closure
01:07

Software Simulation

14 lectures
Introduction to Section 7
01:35
Aspen Plus - Introduction
03:08
Models of Absorption in Aspen Plus
02:18
Case Study 1 - Problem Statement
03:53
Case Study 1 - Simulation & Results
15:00
EXTRA - Case Study 1 - Tray Sizing Effects
03:05
EXTRA - Case Study 1 - Trays vs. Packings
04:19
EXTRA - Case Study 1 - Diluted vs. Concentrated Case
05:19
Aspen HYSYS - Introduction
01:46
Models of Absorption Columns in Aspen HYSYS
03:04
Case Study 2 - Problem Statement
02:39
Case Study 2 - Simulations & Results
07:55
EXTRA - Case Study 2 - Multicomponent Absorption
03:14
Closure - Section 7
01:08

Conclusion

4 lectures
Course Wrap-up
01:39
Conclusion
01:26
Bonus & Surprises!
00:06
Top Unit Operation Q&A
38:22

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